One-Step Preparation and Characterization of Zinc Phosphate Nanocrystals with Modified Surface

نویسندگان

  • Jian Dong Wang
  • Da Li
  • Jin Ku Liu
  • Xiao Hong Yang
  • Jia Luo He
  • Yi Lu
چکیده

The surface-modified zinc phosphate (Zn3(PO4)2) nanocrystals were synthesized by a facile and efficient one-step ultrasonic-template-microwave (UTM) assisted route. The crystal structure, optical properties and morphologies of zinc phosphate nanocrystals were characterized by X-ray diffraction, Fourier transform infrared spectroscopy, Raman spectroscopy and transmission electron microscope. And the TEM image showed that the product had good dispersion with a particle size of 30 35 nm. The anti-corrosion function of anti-corrosive paint using zinc phosphate nanocrystals was researched and the experiment result showed that the salt atmosphere-resistant time was 158 h longer than that of zinc phosphate bulk materials on market. The performance of zinc phosphate nanocrystals with modified surface synthesized by one-step UTM assisted route was improved 63.2% compared with the bulk materials.

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تاریخ انتشار 2011